Iron Oxide Fe3O4 Powder Properties And Preparation
Iron Oxide
Fe3O4 is a substance inorganic with the chemical formula Fe3O4. The magnetic black crystal is called magnetic iron dioxide.
The black Fe3O4 is an iron oxide with mixed valence, melting at 1597degC. It has a density of 5,18g/cm3. Fe3O4 Powder is not soluble with water but is soluble with acid solutions. At room temperature, it appears as magnetite. It is highly conductible and sub-magnetized.
Fe3O4 exhibits anti-corrosion properties. In the case of bluing steel parts, also known as blue-burning or baking blue, an alkaline-oxidizing solution is used to produce a blue-black film of Fe3O4 on the steel surface. Used to improve corrosion resistance, aesthetics and gloss.
1. Precipitation methods
Precipitation, a simple method with low costs, high purity, and uniformity, is a popular method to prepare nanoparticles. This method is also suitable for large-scale manufacturing. The most common precipitation methods are co-precipitation and hydrolytic precipitation. Ultrasonic precipitation is also used, as well as alkoxide hydrogenation and chelate breakdown.
2. Hydrothermal (solvothermal method)
Hydrothermal reaction (solvothermal reaction) is the general term used for chemical reactions which are carried out under high pressure and temperature in fluids, such as aqueous (organic) solvents or steam. The Fe3O4 obtained by the hydrothermal process has a particle size that is small and uniform, it does not need high-temperature pretreatment to calcinate, and it can be doped with multivalent ions.
3. Microemulsification method
The microemulsification technique is the process of creating an emulsion from two immiscible solutions under the influence of surfactants. In this method, amphiphilic molecule divides the continuous medium in tiny spaces that form a small reactor, where the reactants are able to react and form a solid. The microreactor limits the nucleation, growth of crystals, coalescence and agglomeration processes, resulting in nanoparticles which are covered with surfactant, have a certain structure and morphology, and are wrapped.
4. Sol-gel method
The method is based on the hydrolysis of metal alkoxides, followed by polymerization to produce a uniform sol containing metal oxides or hydroxides. They are then concentrated into a clear gel. The gel is dried, and then heat-treated in order to produce superfine powder.
Tech Co., Ltd. is a professional oxide powder We are a chemical product supplier with 12 years of experience. We accept payment by Credit Card, T/T (West Union), Paypal and T/T. The goods will be shipped to overseas customers via FedEx or DHL.
You can contact us for Fe3O4 powder of high quality. Contact us Send an inquiry.
Iron Oxide Fe3O4 Powder Properties
Ferric oxide cannot be dissolved in organic solvents, such as water or alkali solutions. Natural ferroferric dioxide is not soluble when mixed with acid and is readily oxidized into iron oxide (Fe2O3) if the air is humid.The black Fe3O4 is an iron oxide with mixed valence, melting at 1597degC. It has a density of 5,18g/cm3. Fe3O4 Powder is not soluble with water but is soluble with acid solutions. At room temperature, it appears as magnetite. It is highly conductible and sub-magnetized.
Fe3O4 exhibits anti-corrosion properties. In the case of bluing steel parts, also known as blue-burning or baking blue, an alkaline-oxidizing solution is used to produce a blue-black film of Fe3O4 on the steel surface. Used to improve corrosion resistance, aesthetics and gloss.
Iron Oxide Fe3O4 Powder Preparation
The main methods used to prepare nano-Fe3O4 are the hydrothermal method (solvothermal), the microemulsification technique, and the sol-gel technique.1. Precipitation methods
Precipitation, a simple method with low costs, high purity, and uniformity, is a popular method to prepare nanoparticles. This method is also suitable for large-scale manufacturing. The most common precipitation methods are co-precipitation and hydrolytic precipitation. Ultrasonic precipitation is also used, as well as alkoxide hydrogenation and chelate breakdown.
2. Hydrothermal (solvothermal method)
Hydrothermal reaction (solvothermal reaction) is the general term used for chemical reactions which are carried out under high pressure and temperature in fluids, such as aqueous (organic) solvents or steam. The Fe3O4 obtained by the hydrothermal process has a particle size that is small and uniform, it does not need high-temperature pretreatment to calcinate, and it can be doped with multivalent ions.
3. Microemulsification method
The microemulsification technique is the process of creating an emulsion from two immiscible solutions under the influence of surfactants. In this method, amphiphilic molecule divides the continuous medium in tiny spaces that form a small reactor, where the reactants are able to react and form a solid. The microreactor limits the nucleation, growth of crystals, coalescence and agglomeration processes, resulting in nanoparticles which are covered with surfactant, have a certain structure and morphology, and are wrapped.
4. Sol-gel method
The method is based on the hydrolysis of metal alkoxides, followed by polymerization to produce a uniform sol containing metal oxides or hydroxides. They are then concentrated into a clear gel. The gel is dried, and then heat-treated in order to produce superfine powder.
Tech Co., Ltd. is a professional oxide powder We are a chemical product supplier with 12 years of experience. We accept payment by Credit Card, T/T (West Union), Paypal and T/T. The goods will be shipped to overseas customers via FedEx or DHL.
You can contact us for Fe3O4 powder of high quality. Contact us Send an inquiry.
